化学工作者的日常
交流化学知识 提高有机水平
了解一只有机喵的日常生活与工作
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免责声明:本文纯粹基于有机合成学角度对CL-20合成前驱体的合成方法进行简要探讨。本文中所有合成的化合物均不属于含能材料亦无任何可能的被起爆的风险。严禁利用本文所合成的非含能中间体进行含能材料合成实验。严禁未经本人许可对本文截取篡改以及传播。任何私自模仿重复实验的行为及其行为主体应对所面临的风险有清...
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1941年在猫薄荷中分离出荆芥内酯(JACS.1941.63.1558),67-80%猫猫会对其起反应。合成路线如下:(绘图软件:Chemdraw)Step 1.二氧化硒氧化氧化烯丙基位的C-H得到烯丙醇产物反应机理[2,3]σ重排(Ref:J. Org. Chem. 2000, 65, 7554....
在下松田诚一
3年2个月前链接自论坛
内隔热层,材质酚醛树脂测试后可以更换回收,通过对烧蚀程度以及二氧化硅膜厚度和形成情况进行分析。分析硅膜产生情况以及对热效应的影响。石墨喷管降低试验机成本采用石墨喷管,后续会调整为液膜冷却或者循环再生冷却。烧蚀不严重的情况下经氢氟酸浸泡清洗可以复用。套筒固定套,材质316不锈钢用以固定石墨喷管外套桶,...
在下松田诚一
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birch反应是一个很经典的芳烃还原反应(图片来源:有机合成中命名反应的战略性应用反应机理碱金属液氨溶液提供电子,芳环进行单电子转移得到自由基阴离子,然后夺取醇的质子生成自由基,接着自由基在进行一次单电子转移得到碳负离子,再夺取醇的一个质子得到产物。当芳环上有取代基时,还原反应的区域选择性和取代基的...
在下松田诚一
3年2个月前链接自论坛
免责声明:图纸仅供学术研究严禁用于非法用途,持此开源图纸对本项目进行逆向工程、重复实验、技术改进所导致的任何人身伤害及财产损失与本团队无任何关系。保护技术成果,请勿随意传播。任何用此图纸牟利的行为本团队追责到底。本机由XXXXXXXXXXXXXXXXXXXXssago.设计&仿真模拟薛定谔のKN-S...
在下松田诚一
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先上老婆镇楼这是课题里一个片段的第一步反应:(绘图软件:chemdraw)来一篇古早的参考文献反应机理:step1:step2:step3: step4:动力学介导的闭环过渡态(图片来源如下)这是首次报道时的文献给出的过渡态模型(图片来源如下)step5:投料比如下:S.m.1.00 e.q.t...
在下松田诚一
3年3个月前链接自论坛
3,4-Diaminofurazan3,4-二氨基呋扎(3,4-二氨基呋咱)CAS No.:17220-38-1熔点:178-183℃密度:1.582±0.06 g/cm3(Predicted)二氨基呋咱是一种重要的合成砌块,也是优良性能Energetic materials的重要前体。合成方法如下...
在下松田诚一
3年5个月前链接自论坛
采用了发散式合成的方法,首先合成重要砌块2-氨基苯乙酮,然后与芳酰氯进行酰化后分子内缩合得到目标分子(以后有空会做三联苯等诸多用于闪烁体的分子先上方法,实验稍后发
在下松田诚一
3年7个月前链接自论坛
此帖子为预告帖,今年很忙有时间会陆续更新。偏二甲肼是液体火箭发动机的经典燃料,具有比冲高易于引火等诸多优点。但是一般人难以获得,传统制备方法复杂且危险。本人创新合成方法开发出可以大量渐变合成偏二甲肼的绿色化学方法。将在后面的日子里陆续与诸君共赏。传统的合成方法主要有以下三种一,亚硝化还原法此法较为简...
在下松田诚一
3年7个月前链接自论坛
看了好多帖子不少人都认为干燥条件下,五水偶氮四唑钠加热到30°C失去两个结晶水,70°C时成为无水化合物。这是并不正确的,它的来源是以讹传讹。关于偶氮四唑钠的热重分析较为可靠的paper不同温度时偶氮四唑钠盐状态a.五水合物 室温干燥b.二水合物 60度油浴c.五水盐 120度加热d.???150度...
在下松田诚一
3年9个月前链接自论坛
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在下松田诚一
3年10个月前链接自论坛
Evans辅基可以用于手性合成,在不对称合成中应用较为广泛。此次合成手性反应的前体戊酰(R)-(-)苄基Evans后续操作目前无法透露,过一阵子也许可以陆续上传【纯粹是保密而已(笑)】(绘图软件:chemdraw)称取Evans辅剂至于四颈瓶组装好装置,一口装置温度计一口装三通阀中间装恒压漏斗最后一...
在下松田诚一
3年10个月前链接自论坛
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在下松田诚一
3年10个月前链接自论坛
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