化学工作者的日常
交流化学知识 提高有机水平
了解一只有机喵的日常生活与工作
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免责声明：本文纯粹基于有机合成学角度对CL-20合成前驱体的合成方法进行简要探讨。本文中所有合成的化合物均不属于含能材料亦无任何可能的被起爆的风险。严禁利用本文所合成的非含能中间体进行含能材料合成实验。严禁未经本人许可对本文截取篡改以及传播。任何私自模仿重复实验的行为及其行为主体应对所面临的风险有清...
在下松田诚一
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birch反应是一个很经典的芳烃还原反应（图片来源：有机合成中命名反应的战略性应用反应机理碱金属液氨溶液提供电子，芳环进行单电子转移得到自由基阴离子，然后夺取醇的质子生成自由基，接着自由基在进行一次单电子转移得到碳负离子，再夺取醇的一个质子得到产物。当芳环上有取代基时，还原反应的区域选择性和取代基的...
在下松田诚一
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先上老婆镇楼这是课题里一个片段的第一步反应：（绘图软件：chemdraw）来一篇古早的参考文献反应机理：step1：step2：step3： step4：动力学介导的闭环过渡态（图片来源如下）这是首次报道时的文献给出的过渡态模型（图片来源如下）step5：投料比如下：S.m.1.00 e.q.t...
在下松田诚一
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在下松田诚一
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采用了发散式合成的方法，首先合成重要砌块2-氨基苯乙酮，然后与芳酰氯进行酰化后分子内缩合得到目标分子(以后有空会做三联苯等诸多用于闪烁体的分子先上方法，实验稍后发
在下松田诚一
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Mitsunobu反应（光延反应）机理如下我的某中间体由不对称烯丙化产生然而所产生的羟基手性不正确，故用Mitsunobu反应（光延反应）进行羟基翻转（绘图软件：chemdraw）注：所用条件与图示略有不同，不过原理以及方法相同先上试剂全家福（THF为活化分子筛提前2天密封干燥处理后的溶剂）称取1....
在下松田诚一
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在下松田诚一
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在下松田诚一
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