搜索 - 科创网

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内容：引用楼主jn久于发表的 :高氯酸钾是一种相对安全，性能良好的火箭发射药氧化剂，但是这东西真不好买，我跑遍了本地的数十家化试店，均被告知无此品，或许是因为高氯酸钾没有大的工业用途吧。,于是，高氯酸钾的制备提上了我的日程。,方法一：原料：高氯酸，碳酸钾（碳酸氢钾）器材：大烧杯，pH试纸，玻璃 .. (2013-07-13 09:30) 貌似方法三应该是电解氯酸钾

内容：电解制氯酸盐1.制取对象-氯酸钾（1）氯酸钾溶解度随温度变化差异很大（2）氯酸钾在常温时溶解度只有不到十克（3）氯酸钾溶解度小，能够及时转化为沉淀，避免氯酸根再次被电解生成高氯酸根,，污染产品（4）氯酸钾不易吸湿潮解2.电极阳极-石墨阴极-不锈钢或钛阴极主要是防止挥发出的氯化氢或者酸性环境下的氯酸钾和重铬酸钾腐蚀就行3.添加剂石墨作为阳极很容易掉渣，所以需要添加剂-重铬酸钾，他能在石墨表面形成一层铬酸铬保护层,（2）mmo电极可以选择控制温度，因为mmo电极在酸性环境下容易被腐蚀，但是高温时氯酸钾溶解度增大，存在氯酸根，被电解生成高氯酸根，污染产品。

内容：LZ既然问了这个问题而且发在化工版肯定就是希望用化学的办法解决，像RMB法肯定不行，首先氯酸钾价格便宜一般一瓶500g大概10-20元，而高氯酸钾在40左右，相对来说价格太高。,如果LZ的氯酸钾买起来很便宜可以尝试电解氯酸钾，最后生成高氯酸钾和氢气，加热氯酸钾可能会因为一些杂质出现危险而不建议使用，虽然电解法成本低使用方便，但是这个办法对电极有着较高的要求，之前我用铜就被严重腐蚀了

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